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European Congress of Chemical Engineering - 6
Copenhagen 16-21 September 2007

Abstract 1783 - Effects of Synthetic Temperature on the Microstructures and Basic Dyes Adsorption of Titanate Nanotubes

Effects of Synthetic Temperature on the Microstructures and Basic Dyes Adsorption of Titanate Nanotubes

Special Symposium - Environmental Protection & Sustainability

Environmental Protection & Sustainability (EPS - Poster)

Prof Kuen-Song Lin
YUan Ze University
Department of Chemical Engineering & Materials Science
135, Yuan-tong Rd., Chung-Li City, Taiwan.R.O.C.
Taiwan, Province of China

MSc Cheng-Yu Pan
YUan Ze University
Department of Chemical Engineering & Materials Science
135, Yuan-Tong Rd., Chung-Li City, Taiwan, R.O.C.
Taiwan, Province of China

MSc Wen-Ru Chen
Yuan Ze University
Department of Chemical Engineering & Materials Science
135, Yuan-Tong Rd., Cung-Li City, Taiwan, R.O.C.
Taiwan, Province of China

MSc Chih-Ping Liu
Yuan Ze University
Department of Chemical Engineering & Materials Science
135, Yuan-Tong Rd., Cung-Li City, Taiwan, R.O.C.
Taiwan, Province of China

Prof Tsong P. Perng
Yuan Ze University
Department of Chemical Engineering & Materials Science
135, Yuan-Tong Rd., Chung-Li City, Taiwan, R.O.C.
Taiwan, Province of China

Keywords: Titanate nanotube, Synthetic temperature, Nanorod, Basic dyes, Adsorption

Titanate nanotubes were prepared via a hydrothermal treatment of TiO2 powders in a 10 M NaOH solution at 110–270 oC for 24 h. Effects of synthetic temperature on the morphology, phase structure, and pore structure of titanate nanotubes were characterized with TEM, XRD, and nitrogen isotherms, respectively. The adsorption capacity of two basic dyes, Basic Green 5 (BG5) and Basic Violet 10 (BV10), was then measured to identify how the changes of the microstructure affected the basic dyes adsorption characteristics of titanate nanotubes. It was found that when the synthetic temperature was above 160 oC, the microstructure of titanate may transformed from nanotube into nanorod accompanying with the sharp decrease of titanate interlayer spacing, BET surface area, and pore volume. The effects of pore structure variation on the basic dyes adsorption of titanate nanotubes were also discussed.

Presented Monday 17, 13:30 to 15:00, in session Environmental Protection & Sustainability (EPS - Poster) S-7P.

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